反应条件
1: 91 percent / molecular sieves 4 Angstroem; NMO; TPAP / CH2Cl2 / 3 h / 20 °C
2: 68 percent / LHMDS / tetrahydrofuran; hexane / 3 h / -78 - 20 °C
3: 85 percent / HCl / methanol / 10 h / -20 °C
4: 98 percent / triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 °C
5: 97 percent / TBAF / tetrahydrofuran / 3 h / 0 °C
6: 36 percent / Amberlyst 15 / tetrahydrofuran; H2O / 20 h / 20 °C
View Scheme
参考文献
Motoyoshi, Hajime; Horigome, Masato; Watanabe, Hidenori; Kitahara, Takeshi
Tetrahedron, 2006 , vol. 62, # 7 p. 1378 - 1389
