1: 52 percent / SO2Cl2 / hexane; tetrahydrofuran / 3 h / Ambient temperature 2: 90.1 percent / tetrahydrofuran; diethyl ether / 2 h / Ambient temperature 3: 17.6 percent / NaI (8), p-DNB / bis-(2-methoxy-ethyl) ether / 10 h / 80 °C / other or none additive; electron transfer reaction of other polyfluorophenyl pentafluorobenzenesulphonates View Scheme
参考文献
Chen, Qing-Yun; Chen, Ming-Fang
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 7 p. 1071 - 1075
Sethi et al.
Journal of Organometallic Chemistry, 1974 , vol. 69, p. 377
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
Sethi et al.
Journal of Organometallic Chemistry, 1974 , vol. 69, p. 377
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
in tetrahydrofuran
reaction at 0°C, 3 or 16 hours;;
参考文献
Sethi et al.
Journal of Organometallic Chemistry, 1974 , vol. 69, p. 377
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
Tamborski, C.; Moore, G. J.
Journal of Organometallic Chemistry, 1971 , vol. 26, p. 153 - 156
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.2, page 61 - 67
molar ratio of C6F5MgBr to PCl3: 2:1; the main react. is a Cl-Br exchange; small amt. of (C6F5)nPCl(3-n) (n=1,2);
参考文献
Fild, M.; Glemser, O.; Hollenberg, I.
Zeitschrift fuer Naturforschung, 1966 , vol. 21b, p. 920 - 923
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Fild, M.
Diss. Goettingen 1966
