2-羟基-4-异丙基-2H-1,4-噻嗪-3(4H)-酮合成路线 (共 8 条)
反应条件
water in acetone
0.166667 h; Ambient temperature;
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152
反应条件
water in acetone
24 h; Ambient temperature;
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152
反应条件
1: SOCl2, 2,6-lutidine / benzene / 5 h / Ambient temperature
2: 86.2 percent / 0.5 h / Ambient temperature
View Scheme
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152
反应条件
1: SOCl2, 2,6-lutidine / benzene / 5 h / Ambient temperature
2: 83.9 percent / acetone / 0.08 h / Ambient temperature
View Scheme
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152
反应条件
1: SOCl2, 2,6-lutidine / benzene / 5 h / Ambient temperature
2: 92.1 percent / aq. NH3 / acetone / 0.08 h / Ambient temperature
View Scheme
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152
反应条件
1: SOCl2, 2,6-lutidine / benzene / 5 h / Ambient temperature
2: 68.9 percent / CH2Cl2 / 48 h / Ambient temperature
View Scheme
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152
反应条件
2,6-dimethylpyridine; thionyl chloride in benzene
5 h; Ambient temperature; Yield given;
参考文献
Masuda, Ryoichi; Hojo, Masaru; Ichi, Tadaaki; Adachi, Fujio; Yoshinaga, Kenji
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 143 - 152