5-(Z-氨基)-1-戊醇合成路线 （共 12 条）
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water T=0 - 20°C;
参考文献
Journal of the American Chemical Society, , vol. 128, # 12 p. 4058 - 4073
反应条件
triethylsilane; 1,1,1,3,3,3-hexamethyl-disilazane; iron(II) sulfate in dichloromethane T=20°C; 24 h;
参考文献
European Journal of Organic Chemistry, , # 28 p. 4646 - 4650
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=0°C; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2721 - 2730
反应条件
in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Synthesis, , # 9 p. 713 - 716
反应条件
1: 70 percent / pyridine 2: 91 percent / tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 9 p. 713 - 716
反应条件
in tetrahydrofuran T=20°C; Acylation; 19 h;
参考文献
Tetrahedron, , vol. 56, # 43 p. 8433 - 8441
反应条件
1.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere 2.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C / Inert atmosphere 3.1: water; triphenylphosphine / tetrahydrofuran / 10 h / 40 °C / Inert atmosphere 3.2: Inert atmosphere 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2721 - 2730
反应条件
1.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C / Inert atmosphere 2.1: water; triphenylphosphine / tetrahydrofuran / 10 h / 40 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2721 - 2730
反应条件
1.1: water; triphenylphosphine / tetrahydrofuran / 10 h / 40 °C / Inert atmosphere 1.2: Inert atmosphere 2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2721 - 2730
反应条件
1H-imidazole; iodine; triphenylphosphine in dichloromethane 16 h;
参考文献
Zhao, Yingsheng; Chen, Gong
Organic Letters, 2011 , vol. 13, # 18 p. 4850 - 4853
