反应条件
1: 1-n-decyne; dicobalt octacarbonyl; N,N,N'-trimethyl-N'-allylthiourea With 1,1,3,3-tetramethyl-2-thiourea in toluene
Pauson-Khand reaction; 0.0833333 h; Inert atmosphere;
2: carbon monoxide in toluene
T=110°C; Pauson-Khand reaction; P=2250.23 Torr; 22 h; Autoclave;
参考文献
Petrovski, Zeljko; Martins, Bruno M.R.; Afonso, Carlos A.M.
Tetrahedron Letters, 2010 , vol. 51, # 26 p. 3356 - 3359