酞酸-3,4,5,6-d4合成路线 （共 4 条）
反应条件
in methanol; hexane; benzene
参考文献
Ito, Nobuhiro; Esaki, Hiroyoshi; Maesawa, Tsuneaki; Imamiya, Eikoh; Maegawa, Tomohiro; Sajiki, Hironao
Bulletin of the Chemical Society of Japan, 2008 , vol. 81, # 2 p. 278 - 286
反应条件
hydrogen; water-d2; platinum on activated charcoal
T=180°C; 24 h;
参考文献
Sajiki, Hironao; Ito, Nobuhiro; Esaki, Hiroyoshi; Maesawa, Tsuneaki; Maegawa, Tomohiro; Hirota, Kosaku
Tetrahedron Letters, 2005 , vol. 46, # 41 p. 6995 - 6998
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 15 h / Reflux
2: phosphorus tribromide / dichloromethane / 2 h / 20 °C
3: lithium / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere; Sonication
View Scheme
参考文献
Hamza, Abdulhamid
Structural Chemistry, 2010 , vol. 21, # 4 p. 787 - 793
反应条件
acetic anhydride in dichloromethane
3 h; Reflux;
参考文献
Verbeeck, Stefan; Herrebout, Wouter A.; Gulevskaya, Anna V.; Van Der Veken, Benjamin J.; Maes, Bert U. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5126 - 5133
