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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
87976-36-1
合成路线
（共 9 条）
259268-77-4
→
反应条件
87976-36-1
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Danilov; Balagurova; Vinnikova; Utkina; Torgov; Kalinchuk; Druzhinina; Veselovsky
Russian Journal of Bioorganic Chemistry, 2014 , vol. 40, # 1 p. 89 - 96
Biokhimiya (Moscow), 2014 , vol. 40, # 1 p. 99 - 107
201230-82-2
→
反应条件
87976-36-1
反应条件
[Rh(acac)2(CO)2]; polyoxyethanyl α-tocopheryl sebacate; hydrogen; 6-DPPon in water T=20°C; P=760.051 Torr; 24 h; Schlenk technique; regioselective reaction;
参考文献
Straub, Alexander T.; Otto, Marina; Usui, Ippei; Breit, Bernhard
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2071 - 2075
65-85-0
苯甲酸
→
反应条件
87976-36-1
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 3.5 h / 20 - 50 °C / |Inert atmosphere 2: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Danilov; Balagurova; Vinnikova; Utkina; Torgov; Kalinchuk; Druzhinina; Veselovsky
Russian Journal of Bioorganic Chemistry, 2014 , vol. 40, # 1 p. 89 - 96
Biokhimiya (Moscow), 2014 , vol. 40, # 1 p. 99 - 107
1611-56-9
11-溴-1-十一醇
→
反应条件
87976-36-1
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 3.5 h / 20 - 50 °C / |Inert atmosphere 2: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Danilov; Balagurova; Vinnikova; Utkina; Torgov; Kalinchuk; Druzhinina; Veselovsky
Russian Journal of Bioorganic Chemistry, 2014 , vol. 40, # 1 p. 89 - 96
Biokhimiya (Moscow), 2014 , vol. 40, # 1 p. 99 - 107
98-88-4
苯甲酰氯
→
反应条件
87976-36-1
反应条件
1.1: pyridine / dichloromethane / 4 h / 20 °C 2.1: boron trifluoride diethyl etherate; sodium tetrahydroborate / tetrahydrofuran / 1.5 h / |Inert atmosphere 2.2: 18 h / -10 °C / |Inert atmosphere 3.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Danilov; Balagurova; Vinnikova; Utkina; Torgov; Kalinchuk; Druzhinina; Veselovsky
Russian Journal of Bioorganic Chemistry, 2014 , vol. 40, # 1 p. 89 - 96
Biokhimiya (Moscow), 2014 , vol. 40, # 1 p. 99 - 107
112-43-6
10-十一烯-1-醇
→
反应条件
87976-36-1
反应条件
1.1: pyridine / dichloromethane / 4 h / 20 °C 2.1: boron trifluoride diethyl etherate; sodium tetrahydroborate / tetrahydrofuran / 1.5 h / |Inert atmosphere 2.2: 18 h / -10 °C / |Inert atmosphere 3.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Danilov; Balagurova; Vinnikova; Utkina; Torgov; Kalinchuk; Druzhinina; Veselovsky
Russian Journal of Bioorganic Chemistry, 2014 , vol. 40, # 1 p. 89 - 96
Biokhimiya (Moscow), 2014 , vol. 40, # 1 p. 99 - 107
96042-20-5
→
反应条件
87976-36-1
反应条件
1.1: boron trifluoride diethyl etherate; sodium tetrahydroborate / tetrahydrofuran / 1.5 h / |Inert atmosphere 1.2: 18 h / -10 °C / |Inert atmosphere 2.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Danilov; Balagurova; Vinnikova; Utkina; Torgov; Kalinchuk; Druzhinina; Veselovsky
Russian Journal of Bioorganic Chemistry, 2014 , vol. 40, # 1 p. 89 - 96
Biokhimiya (Moscow), 2014 , vol. 40, # 1 p. 99 - 107
112-45-8
10-十一烯醛
+
98-88-4
苯甲酰氯
→
反应条件
87976-36-1
反应条件
Yield given. Multistep reaction;
参考文献
Hodge, Philip; Waterhouse, Janette
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2319 - 2323
87976-36-1
→
反应条件
80158-99-2
反应条件
diethyl ether; methyllithium in tetrahydrofuran T=20°C; 6 h;
参考文献
ISHIHARA SANGYO KAISHA, LTD.
Patent: WO2004/52872 A1, 2004 ;
Location in patent: Page 54-55 ;
