2,4,6-三甲基苯胺合成路线 (共 254 条)
反应条件
2-((dicyclohexylphosphino)methyl)-1,3-bis(2,6-diisopropylphenyl)-4,5-dimethyl-1H-imidazol-3-ium iodide; ammonia; palladium diacetate; sodium t-butanolate in 1,4-dioxane T=120°C; P=7500.75 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 35 p. 9599 - 9604
反应条件
copper(I) oxide; ammonium hydroxide; air in methanol T=20°C; 12 h;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 6 p. 1114 - 1116
反应条件
Pd[P(o-tol)3]2; CyPF-t-Bu; ammonia; sodium t-butanolate in 1,4-dioxane T=50°C; 24 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 31 p. 11049 - 11061
反应条件
palladium 10 on activated carbon; hydrogen in tetrahydrofuran 12 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 30 p. 12354 - 12357
反应条件
ammonium hydroxide; potassium phosphate; 1-(5,6,7,8-tetrahydroquinolin-8-yl)-2-methylpropan-1-one; copper(I) bromide in dimethyl sulfoxide T=80°C; 24 h; Inert atmosphereSealed tube;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 11-12 p. 1722 - 1726
反应条件
16-crown-6; 1-aminoquinolinium perchlorate in trifluoroacetic acid 4 h; Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 6 p. 1525 - 1529
反应条件
sodium dithionite in methanol; dichloromethane; water 3 h; Heating;
参考文献
Synlett, , # 11 p. 1695 - 1698
反应条件
1: 59 percent / 3 h / Ambient temperature 2: 43 percent / HN3, H2SO4 / CHCl3 / 20 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 116, # 3 p. 1016 - 1026
反应条件
ammonia; KNH2 T=-33°C; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 102, # 24 p. 7375 - 7377
反应条件
ammonia; KNH2 T=-33°C; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 102, # 24 p. 7375 - 7377