2,4,6-三甲基苯胺合成路线 (共 254 条)
反应条件
tributylphosphine; di-isopropyl azodicarboxylate in dichloromethane T=-78 - 20°C; P=760 Torr;
参考文献
Saylik, Dilek; Horvath, Michael J.; Elmes, Patricia S.; Jackson, W. Roy; Lovel, Craig G.; Moody, Keith
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3940 - 3946
反应条件
triphenylphosphine in dichloromethane T=-78 - 20°C; P=760 Torr;
参考文献
Journal of Organic Chemistry, , vol. 64, # 11 p. 3940 - 3946
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=25°C; 0.166667 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias; Schlechtingen, Georg
Angewandte Chemie, 1995 , vol. 107, # 22 p. 2746 - 2749
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=82°C; 18 h;
参考文献
Angewandte Chemie, , vol. 107, # 22 p. 2746 - 2749
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=25°C; 4 h;
参考文献
Angewandte Chemie, , vol. 107, # 22 p. 2746 - 2749
反应条件
2: 75 percent / DBU / dimethylsulfoxide / Ambient temperature View Scheme
参考文献
Eisenberg
Chemische Berichte, 1882 , vol. 15, p. 1018
参考文献
Habib, Nargues S.; Rieker, Anton
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 11 p. 1593 - 1597
反应条件
in ethyl acetate 1.) 40 - 50 deg C, 1 h, 2.) 80 deg C, 2 h;
参考文献
Reidemeister; Stark, Holger; Ligneau; Ganellin; Schwartz; Schunack
Pharmazie, 2000 , vol. 55, # 2 p. 83 - 86
参考文献
Siefken
Justus Liebigs Annalen der Chemie, 1949 , vol. 562, p. 75,1114
反应条件
hydrogenchloride durch Bromieren;
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4418208 A1, 1983 ;