2,4,6-三甲基苯胺合成路线 （共 254 条）
反应条件
in dichloromethane T=40°C; 10 h;
参考文献
Yang, Dan; Chen, Ying-Chun; Zhu, Nian-Yong
Organic Letters, 2004 , vol. 6, # 10 p. 1577 - 1580
参考文献
Beck, James P.; Curry, Matt A.; Chorvat, Robert J.; Fitzgerald, Larry W.; Gilligan, Paul J.; Zaczek, Robert; Trainor, George L.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 8 p. 1185 - 1188
反应条件
1: diethyl ether / 2 - 5 °C 2: Et3N; EtOCOCl / CHCl3 / -10 - 20 °C View Scheme
参考文献
Eisenberg
Chemische Berichte, 1882 , vol. 15, p. 1018
参考文献
Habib, Nargues S.; Rieker, Anton
Synthesis, 1984 , # 10 p. 825 - 827
参考文献
Eisenberg
Chemische Berichte, 1882 , vol. 15, p. 1018
反应条件
pyridine in dichloromethane T=0 - 20°C; 12 h;
参考文献
Uyanik, Muhammet; Yasui, Takeshi; Ishihara, Kazuaki
Tetrahedron, 2010 , vol. 66, # 31 p. 5841 - 5851
反应条件
2-hydroxypropionic acid; boric acid trimethyl ester; 2,3-dihydro-1,4-dihydroxyanthraquinone T=50 - 145°C; 4.5 h; Product distribution / selectivity;
参考文献
LANXESS Deutschland GmbH
Patent: US2008/139830 A1, 2008 ;
Location in patent: Page/Page column 4 ;
反应条件
weiteres Edukt: 2,4,6-Trimethyl-anilin-hydrochlorid;
参考文献
Dokunichin; Kurdjumowa
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 617,621; engl. Ausg. S. 589, 591
反应条件
1: toluene / Heating 2: LiAlH4 / diethyl ether; tetrahydrofuran View Scheme
参考文献
Dallacker,F.; Eschelbach,F.-E.
Justus Liebigs Annalen der Chemie, 1965 , vol. 689, p. 171 - 178
参考文献
Ullmann
Justus Liebigs Annalen der Chemie, 1903 , vol. 327, p. 110
