N,N-二乙基氯甲酰胺合成路线 （共 193 条）
反应条件
1: phenyllithium With CuCN in diethyl ether T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in diethyl ether T=-30 - 20°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
1: 0.08 h / Heating 2: 95 percent / NiCl2(PPh3)2 / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Lemoucheux; Rouden; Lasne
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9997 - 10001
反应条件
triethylamine in dichloromethane T=0 - 20°C;
参考文献
El-Faham, Ayman; Khattab, Sherine N.; Abdul-Ghani, Mohamed; Albericio, Fernando
European Journal of Organic Chemistry, 2006 , # 6 p. 1563 - 1573
反应条件
1: phenyllithium With CuCN in diethyl ether T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in diethyl ether T=-30 - 20°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
1: n-butyllithium With CuCN in tetrahydrofuran T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in tetrahydrofuran T=-30 - 0°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
1: tert.-butyl lithium With CuCN in tetrahydrofuran T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in tetrahydrofuran T=-30 - 0°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
1: tert.-butyl lithium With CuCN in diethyl ether T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in diethyl ether T=-30 - 0°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
triethylamine T=20°C; 0.333333 h;
参考文献
DIRECTOR GENERAL, DEFENCE RESEARCH and DEVELOPMENT ORGANISATION; RAO, Ambati Narasimha; GANESAN, Kumaran; VIJAYARAGHAVAN, Rajagopalan
Patent: WO2013/65059 A1, 2013 ;
Location in patent: Page/Page column 13 ;
反应条件
1: 88 percent / sodium hydride / tetrahydrofuran / 20 °C 2: N,N,N,N-tetramethylenediamine; s-butyllithium / tetrahydrofuran / 16 h / 20 °C 3: 1.57 g / potassium carbonate View Scheme
参考文献
Kamila, Sukanta; Mukherjee, Chandrani; Mondal, Sasanka S.; De, Asish
Tetrahedron, 2003 , vol. 59, # 8 p. 1339 - 1348
参考文献
Lustig,E. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 851 - 852
