N,N-二乙基氯甲酰胺合成路线 （共 193 条）
参考文献
Lumiere; Perrin
Bulletin de la Societe Chimique de France, 1904 , vol. <3> 31, p. 691
反应条件
1: sec.-butyllithium With CuCN in tetrahydrofuran T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in tetrahydrofuran T=-30 - 0°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
1: tert.-butyl lithium With CuCN in diethyl ether T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in diethyl ether T=-30 - 0°C; 2 h;
参考文献
Organic Letters, , vol. 6, # 21 p. 3703 - 3706
反应条件
1: 1) NaH / DMF, 0 deg C up to r.t. 2: 1) LDA / 1) THF, -78 deg C View Scheme
参考文献
Lee, John; Tsukazaki, Masao; Snieckus, Victor
Tetrahedron Letters, 1993 , vol. 34, # 3 p. 415 - 418
参考文献
Hudson,R.F. et al.
Helvetica Chimica Acta, 1967 , vol. 50, p. 997 - 1002
反应条件
3: 71 percent / 28percent aq. NH4OH / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Desai; Hlasta; Monsour; Saindane
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7161 - 7163
参考文献
Reetz et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 3813,3815
Full Text Show Details
Arbusow; Rispoloshenskii
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1952 , p. 854,859;engl.Ausg.S.765,769
参考文献
Herize, Armando; Dominguez, Rosa M.; Rotinov, Alexandra; Nunez, Oswaldo; Chuchani, Gabriel
Journal of Physical Organic Chemistry, 1999 , vol. 12, # 3 p. 201 - 206
反应条件
1: tert.-butyl lithium With CuCN in diethyl ether T=-30°C; 0.5 h; 2: N,N-diethyl carbamoyl chloride in diethyl ether T=-30 - 0°C; 2 h;
参考文献
Lemoucheux, Laurent; Seitz, Thomas; Rouden, Jacques; Lasne, Marie-Claire
Organic Letters, 2004 , vol. 6, # 21 p. 3703 - 3706
反应条件
Yield given. Multistep reaction;
参考文献
Hiiro, Tomoki; Mogami, Toshiaki; Kambe, Nobuaki; Fujiwara, Shin-Ichi; Sonoda, Noboru
Synthetic Communications, 1990 , vol. 20, # 5 p. 703 - 711
