N,N-二乙基氯甲酰胺合成路线 （共 193 条）
参考文献
Winthrop Chem. Co.
Patent: US2209245 , 1938 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE709941 , 1937 ;
DRP/DRBP Org.Chem.
反应条件
1-methyl-1H-imidazole T=20°C; 0.5 h;
参考文献
DIRECTOR GENERAL, DEFENCE RESEARCH and DEVELOPMENT ORGANISATION; RAO, Ambati Narasimha; GANESAN, Kumaran; VIJAYARAGHAVAN, Rajagopalan
Patent: WO2013/65059 A1, 2013 ;
Location in patent: Page/Page column 12 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 24 h; Reflux;
参考文献
Rieke, Reuben D.; Kim, Seung-Hoi
Tetrahedron Letters, 2012 , vol. 53, # 27 p. 3478 - 3481
参考文献
Tilles
Journal of the American Chemical Society, 1959 , vol. 81, p. 714,716
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Stepanova, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 6 p. 1115 - 1119
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1287 - 1291
反应条件
aluminium trichloride T=175 - 180°C; 3 h; changing amount of catalyst, temperature, and time; Product distribution;
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Stepanova, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 6 p. 1115 - 1119
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1287 - 1291
反应条件
tin(IV) chloride 3 h; Heatingchanging amount of catalyst, temperature, and time; Product distribution;
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Stepanova, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 6 p. 1115 - 1119
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1287 - 1291
反应条件
1: 1.) NaH, 2.) DMAP / 1.) THF, 0 deg C, 2.) THF, 0 deg C to room temp., 20 h 2: 70 percent / K2CO3, CuO / dimethylformamide / 1.5 h / Heating 3: 58 percent / TMEDA, sec-BuLi / tetrahydrofuran; cyclohexane / -78 deg C to room temp., then overnight View Scheme
参考文献
Danishefsky; Lee
Journal of the American Chemical Society, 1989 , vol. 111, # 13 p. 4829 - 4837
反应条件
1: iPr2NEt; DMAP / CH2Cl2 2: TFA / CH2Cl2 View Scheme
参考文献
Fujii et al.
Yakugaku Zasshi, 1954 , vol. 74, p. 1049
Chem.Abstr., 1955 , p. 11666
参考文献
Kushner et al.
Journal of Organic Chemistry, 1948 , vol. 13, p. 144,149
