反应条件
1: 100 percent / i-Pr2NEt / CH2Cl2 / cooling
2: 98 percent / NCS / tetrahydrofuran / 1 h / -10 °C
3: 77 percent / aqueous HF / acetonitrile / 2 h
4: 68 percent / HCOOH; Et3N / [RuCl2(η6-p-cymene)]2; (1R,2R)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine / dimethylformamide / 1.25 h / 20 °C
View Scheme
参考文献
Tanis, Steven P.; Evans, Bruce R.; Nieman, James A.; Parker, Timothy T.; Taylor, Wendy D.; Heasley, Steven E.; Herrinton, Paul M.; Perrault, William R.; Hohler, Richard A.; Dolak, Lester A.; Hester, Matthew R.; Seest, Eric P.
Tetrahedron Asymmetry, 2006 , vol. 17, # 14 p. 2154 - 2182
