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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻溴苯甲酸
合成路线
（共 376 条）
88-65-3
邻溴苯甲酸
→
反应条件
610-71-9
2,5-二溴苯甲酸
反应条件
water; bromine T=150 - 160°C;
参考文献
Banerjee, Amalendu; Banerjee, Gopal Chandra; Dutt, Sachchidananda; Banerjee, Santa (Mrs.); Samaddar, Haraprasad
Journal of the Indian Chemical Society, 1980 , vol. 57, # 6 p. 640 - 642
88-65-3
邻溴苯甲酸
→
反应条件
5411-56-3
1-(2-溴苯基)乙醇
反应条件
1: thionyl chloride / diethyl ether / 2 h / Reflux 2: iron (III) acetylacetonate / diethyl ether / -78 °C / Inert atmosphere 3: Candida tenuis AKR2B5 xylose reductase [E.(1)C11175]; water; Reduced nicotinamide-adenine dinucleotide / ethanol / 25 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Vogl, Michael; Kratzer, Regina; Nidetzky, Bernd; Brecker, Lothar
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 16 p. 5863 - 5870
88-65-3
邻溴苯甲酸
→
反应条件
61436-88-2
2-溴-N-甲基苯甲酰胺
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice View Scheme
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
74-89-5
甲胺
+
88-65-3
邻溴苯甲酸
→
反应条件
61436-88-2
2-溴-N-甲基苯甲酰胺
反应条件
thionyl chloride 2.) water; Yield given. Multistep reaction;
参考文献
Ohkata, Katsuo; Ohnishi, Masako; Akiba, Kin-ya
Tetrahedron Letters, 1988 , vol. 29, # 42 p. 5401 - 5404
88-65-3
邻溴苯甲酸
→
反应条件
1338259-06-5
反应条件
1.1: dicyclohexyl-carbodiimide / 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 h / 20 °C / Inert atmosphere 2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 0.67 h / 100 °C / Sealed vial 3.1: 2,2'-azo-bisisobutyronitrile; N-bromosuccinmide / tetrachloromethane / 2 h / 100 °C 4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere 4.2: 1 h / 0 - 20 °C 5.1: sodium hydroxide / ethanol / 2 h / 100 °C 5.2: 20 °C / pH ~ 4 6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.08 h 6.2: 0.5 h / 20 °C 7.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C View Scheme
参考文献
SCRIPPS RESEARCH INSTITUTE, THE
Patent: US2012/309757 A1, 2012 ;
80-10-4
二苯二氯硅烷
+
88-65-3
邻溴苯甲酸
→
反应条件
129459-84-3
反应条件
in benzene T=-20°C; 6 h;
参考文献
Dzhuraev, A. D.; Karimuklov, K. M.; Makhsumov, A. G.; Zakirov, U. B.; Radzhabova, Sh. D.; Tsinzadze, N. Kh.
Pharmaceutical Chemistry Journal, 1990 , vol. 24, # 6 p. 422 - 424
Khimiko-Farmatsevticheskii Zhurnal, 1990 , vol. 24, # 6 p. 33 - 34
88-65-3
邻溴苯甲酸
→
反应条件
131118-02-0
2-溴-2’-甲氧基苯甲酮
反应条件
1: 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide / acetonitrile / 4 h / 0 - 23 °C 2: trifuran-2-yl-phosphane; bis(dibenzylideneacetone)-palladium(0) / toluene / 23 °C / Inert atmosphere View Scheme
参考文献
Kunchithapatham, Kamala; Eichman, Chad C.; Stambuli, James P.
Chemical Communications, 2011 , vol. 47, # 47 p. 12679 - 12681
88-65-3
邻溴苯甲酸
→
反应条件
13161-80-3
反应条件
1: (i) Cu, K2CO3, pentane-1-ol, (ii) polyphosphoric acid 2: K2CO3 / acetone View Scheme
参考文献
Beck; Kwok; Booher; Brown; Patterson; Pranc; Rockey; Pohland
Journal of the American Chemical Society, 1968 , vol. 90, # 17 p. 4706 - 4710
88-65-3
邻溴苯甲酸
→
反应条件
5411-56-3
1-(2-溴苯基)乙醇
反应条件
1: thionyl chloride / diethyl ether / 2 h / Reflux 2: iron (III) acetylacetonate / diethyl ether / -78 °C / Inert atmosphere 3: Candida tenuis AKR2B5 xylose reductase [E.(1)C11175]; water; Reduced nicotinamide-adenine dinucleotide / ethanol / 25 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Vogl, Michael; Kratzer, Regina; Nidetzky, Bernd; Brecker, Lothar
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 16 p. 5863 - 5870
95-51-2
邻氯苯胺
+
88-65-3
邻溴苯甲酸
→
反应条件
10166-39-9
N-(2-氯苯基)邻氨基苯甲酸
反应条件
4-methyl-morpholine; copper(I) oxide in 1,4-dioxane 16 h; Heating;
参考文献
Chalmers; Scholz; Topliss; Kolliniatis; Munro; Craik; Iskander; Stockigt
Journal of Medicinal Chemistry, 1993 , vol. 36, # 9 p. 1272 - 1277
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