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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻溴苯甲酸
合成路线
（共 376 条）
88-65-3
邻溴苯甲酸
→
反应条件
61593-14-4
反应条件
1.1: oxalyl chloride / CH2Cl2; dimethylformamide / 4 h / 20 °C 2.1: CuCN*2LiCl / tetrahydrofuran / 0.25 h / -40 °C 2.2: 76 percent / tetrahydrofuran / -40 - -5 °C View Scheme
参考文献
Cahiez, Gerard; Luart, Denis; Lecomte, Fabien
Organic Letters, 2004 , vol. 6, # 24 p. 4395 - 4398
88-65-3
邻溴苯甲酸
→
反应条件
61762-84-3
反应条件
1: potassium carbonate; copper; isoamyl alcohol 2: carbon disulfide; phosphorus (V)-chloride View Scheme
参考文献
Graves et al.
Journal and Proceedings of the Royal Society of New South Wales, 1938 , vol. 71, p. 255,257
88-65-3
邻溴苯甲酸
→
反应条件
62220-51-3
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
88-65-3
邻溴苯甲酸
→
反应条件
62220-52-4
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating 4: 37 percent / KOH / ethanol / 96 h / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
88-65-3
邻溴苯甲酸
→
反应条件
62220-53-5
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating 4: 37 percent / KOH / ethanol / 96 h / Ambient temperature 5: 20.1 g / thionyl chloride View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
88-65-3
邻溴苯甲酸
→
反应条件
62220-54-6
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating 4: 37 percent / KOH / ethanol / 96 h / Ambient temperature 5: 20.1 g / thionyl chloride 6: 27.0 g / dioxane; H2O / 1 h View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
88-65-3
邻溴苯甲酸
→
反应条件
62220-56-8
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating 4: 37 percent / KOH / ethanol / 96 h / Ambient temperature 5: 20.1 g / thionyl chloride 6: 96 percent / dioxane; H2O / 1 h View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
88-65-3
邻溴苯甲酸
→
反应条件
62220-57-9
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating 4: 37 percent / KOH / ethanol / 96 h / Ambient temperature 5: 20.1 g / thionyl chloride 6: 27.0 g / dioxane; H2O / 1 h 7: LiAlH4 / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
88-65-3
邻溴苯甲酸
→
反应条件
62220-62-6
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating 4: 37 percent / KOH / ethanol / 96 h / Ambient temperature 5: 20.1 g / thionyl chloride 6: 98 percent / triethylamine / acetonitrile / 3 h / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
88-65-3
邻溴苯甲酸
→
反应条件
62220-63-7
反应条件
1: 96 percent / potassium carbonate, powdered copper / H2O / 3 h / 130 - 140 °C 2: thionyl chloride / 5 h / 60 °C 3: 0.5 h / Heating 4: 37 percent / KOH / ethanol / 96 h / Ambient temperature 5: 20.1 g / thionyl chloride 6: triethylamine / acetonitrile / 3 h / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
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