反应条件
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 12 h / 20 °C / |Inert atmosphere
2.1: copper(l) iodide; triphenylphosphine / tetrahydrofuran / |Inert atmosphere
2.2: 12 h / 20 °C / |Inert atmosphere
3.1: hydrogen tetrachloroaurate(III) trihydrate; water / acetonitrile / 1 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Patil, Nitin T.; Shinde, Valmik S.; Thakare, Milind S.; Hemant Kumar; Bangal, Prakriti. R.; Barui, Ayan Kumar; Patra, Chitta Ranjan
Chemical Communications, 2012 , vol. 48, # 91 p. 11229 - 11231