2,4,6-三硝基氯苯合成路线 （共 249 条）
反应条件
2: aq. HClO4 / dioxane
View Scheme
参考文献
Tamura; Minamikawa; Sumoto; Fujii; Ikeda
The Journal of organic chemistry, 1973 , vol. 38, # 6 p. 1239 - 1241
反应条件
in ethanol
6 h; Reflux;
参考文献
Badgujar; Talawar; Asthana; Mahulikar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2010 , vol. 49, # 12 p. 1675 - 1677
反应条件
in ethanol; water
excess of NaHSO3 soln.;
参考文献
Gmelin Handbook: S: MVol.B2, 3.1.3, page 603 - 607
反应条件
1: Na2S2O5 / ethanol
3: 190 °C
View Scheme
参考文献
Pettitt,D.J.; Helmkamp,G.K.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2702 - 2706
反应条件
in dimethyl sulfoxide
参考文献
Sekiguchi, Shizen; Ishikura, Hiromi; Hirosawa, Yukitoshi; Ono, Nobuyuki
Tetrahedron, 1990 , vol. 46, # 16 p. 5567 - 5578
反应条件
1: 76 percent / dimethylsulfoxide / 3 h / 30 °C / or 2h, 50 deg C
2: 56 percent / dimethylsulfoxide / 0.05 h / 30 °C
View Scheme
参考文献
Sekiguchi, Shizen; Ishikura, Hiromi; Hirosawa, Yukitoshi; Ono, Nobuyuki
Tetrahedron, 1990 , vol. 46, # 16 p. 5567 - 5578
参考文献
Bernasconi,C.F. et al.
Journal of Organic Chemistry, 1973 , vol. 38, p. 2838 - 2842
参考文献
Crampton, Michael R.; Holmes, Anthony J.
Journal of Physical Organic Chemistry, 1998 , vol. 11, # 11 p. 787 - 792
反应条件
in 1,4-dioxane
1 h; Ambient temperature;
参考文献
Mel'nikov, A. I.; Gitis, S. S.; Kaminskii, A. Ya.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 7 p. 1336 - 1343
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 7 p. 1486 - 1494
反应条件
1: 77 percent / dioxane; various solvent(s)
2: conc. H2SO4 / acetonitrile
View Scheme
参考文献
Mel'nikov, A. I.; Gitis, S. S.; Kaminskii, A. Ya.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 10 p. 1931 - 1932
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 10 p. 2217 - 2218
