4-环己烯-1,2-二羧酸合成路线 (共 12 条)
反应条件
1.1: palladium; hydrogen / methanol / 30 - 35 °C 2.1: ethanol / 30 h / 35 - 75 °C 2.2: 1 h 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 65 °C 4.1: triethylamine / dichloromethane / 0.42 h / 25 - 35 °C / |Inert atmosphere 4.2: 3 h / -5 - 35 °C View Scheme
参考文献
CADILA HEALTHCARE LIMITED; DWIVEDI, Shri Prakash Dhar; SINGH, Ramesh Chandra; CHAVDA, Rajendra Gokalbhai
Patent: WO2013/121440 A1, 2013 ;
反应条件
peracetic acid; acetone
参考文献
Union Carbide and Carbon Corp.
Patent: US2794028 , 1953 ;