反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice 2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere 3.1: silica gel; pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere 4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere 4.2: -78 - 20 °C / Inert atmosphere 5.1: methanol; acetyl chloride / 20 °C / Inert atmosphere 6.1: silica gel; pyridinium chlorochromate / dichloromethane / Inert atmosphere View Scheme
参考文献
Xia, Wujiong; Shao, Yutian; Gui, Weijun; Yang, Chao
Chemical Communications, 2011 , vol. 47, # 39 p. 11098 - 11100
