反应条件
1: 1,2-benzenedicarboxylic acid; Wang resin With di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=0 - 20°C; 24 h;
2: n-Octylamine With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
18 h;
3: in N,N-dimethyl-formamide
0.333333 h; microwave irradiation;
参考文献
Martin, Benedicte; Sekljic, Harald; Chassaing, Christophe
Organic Letters, 2003 , vol. 5, # 11 p. 1851 - 1853
