反应条件
1: 1.) oxalyl chloride, 2.) triethylamine / 1.) benzene/DMF, r.t., 2 h, 2.) THF, 1 h
2: 74 percent / LiAlH4 / tetrahydrofuran / Heating
3: 84 percent / nitrosation
4: 67 percent / LiAlH4
5: 25 percent / HgO
View Scheme
参考文献
Newcomb,M.; Burchill,Mt.; Deeb,T.M.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6528
