5-叔丁基-2-甲氧基-苯磺酰氯合成路线 （共 3 条）
反应条件
chlorosulfonic acid in dichloromethane
a) from 0 deg C to 5 deg C, 1 h, b) RT, 1 h;
参考文献
Drygala; Kirby; Watson
Synthetic Communications, 1994 , vol. 24, # 5 p. 671 - 675
反应条件
1: 60 percent / aq. NH3 / acetonitrile / 16 h / Ambient temperature
2: 95 percent / AlCl3 / xylene / 24 h / 55 - 60 °C
View Scheme
参考文献
Drygala; Kirby; Watson
Synthetic Communications, 1994 , vol. 24, # 5 p. 671 - 675
反应条件
ammonium hydroxide in acetonitrile
16 h; Ambient temperature;
参考文献
Drygala; Kirby; Watson
Synthetic Communications, 1994 , vol. 24, # 5 p. 671 - 675
