反应条件
1: 1.) NaH, NaI / 1.) liq. paraffin, 1,2-dimethoxyethane, 4 deg C, 30 min, 2.) liq. paraffin, 1,2-dimethoxyethane, RT, 6 h
2: SO2Cl2 / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
参考文献
Benneche, T; Strande, P; Oftebro, R; Undheim, K
European Journal of Medicinal Chemistry, 1993 , vol. 28, # 6 p. 463 - 472