lithium aluminium tetrahydride in tetrahydrofuran Heating;

1: 64 percent / H2 / 10percent Pd/C / ethanol; acetic acid; ethyl acetate / 0.75 h / 2068.6 - 2844.3 Torr 2: diethyl ether / 0.5 h / 0 °C 3: 41 percent / tetrahydrofuran; diethyl ether / 0 °C / pH > 9 4: 58 percent / LiAlH4 / tetrahydrofuran / Heating View Scheme

1: diethyl ether / 0.5 h / 0 °C 2: 41 percent / tetrahydrofuran; diethyl ether / 0 °C / pH > 9 3: 58 percent / LiAlH4 / tetrahydrofuran / Heating View Scheme

1: 41 percent / tetrahydrofuran; diethyl ether / 0 °C / pH > 9 2: 58 percent / LiAlH4 / tetrahydrofuran / Heating View Scheme