反应条件
1: 1. chlorine / 1. 60 deg C, 1 h 2. DMF, reflux, 2 h
2: 1. NaH 2. NaBH4, glacial HOAc / 1. ether, a) reflux b) cooling (ice-water) c) reflux, 10 min
View Scheme
参考文献
Carpino, Louis A.; Cohen, Beri J.; Lin, Yao-Zhong; Stephens, Kenton E.; Triolo, Salvatore
Journal of Organic Chemistry, 1990 , vol. 55, # 1 p. 251 - 259
