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63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88105-10-6
合成路线
（共 9 条）
111828-30-9
→
反应条件
88105-10-6
+
111828-38-7
反应条件
toluene-4-sulfonic acid in ethanol 2.5 h; Heating;
参考文献
Takagi, Kaname; Aotsuka, Tomoji; Morita, Hikari; Okamoto, Yoshihisa
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1443 - 1449
88105-08-2
→
反应条件
88105-10-6
反应条件
hydrogenchloride; sodium carbonate 1 h;
参考文献
Okamoto, Yoshihisa; Ueda, Takeo; Takagi, Kaname
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2114 - 2119
42510-46-3
→
反应条件
88105-10-6
反应条件
1: 90.9 percent / H2O / 2 h 2: 80 percent / NaOH / H2O / 2.5 h / Heating 3: 69.3 percent / 1percent HCl, 10percent sodium carbonate / 1 h View Scheme
参考文献
Okamoto, Yoshihisa; Ueda, Takeo; Takagi, Kaname
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2114 - 2119
88105-03-7
→
反应条件
88105-10-6
反应条件
1: 72.5 percent / 10percent HCl / ethanol / 0.08 h 2: 90.9 percent / H2O / 2 h 3: 80 percent / NaOH / H2O / 2.5 h / Heating 4: 69.3 percent / 1percent HCl, 10percent sodium carbonate / 1 h View Scheme
参考文献
Okamoto, Yoshihisa; Ueda, Takeo; Takagi, Kaname
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2114 - 2119
88105-06-0
→
反应条件
88105-10-6
反应条件
1: 38 percent / 10percent HCl / H2O / 0.05 h 2: 90.9 percent / H2O / 2 h 3: 80 percent / NaOH / H2O / 2.5 h / Heating 4: 69.3 percent / 1percent HCl, 10percent sodium carbonate / 1 h View Scheme
参考文献
Okamoto, Yoshihisa; Ueda, Takeo; Takagi, Kaname
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2114 - 2119
88105-04-8
→
反应条件
88105-10-6
反应条件
1: 80 percent / NaOH / H2O / 2.5 h / Heating 2: 69.3 percent / 1percent HCl, 10percent sodium carbonate / 1 h View Scheme
参考文献
Okamoto, Yoshihisa; Ueda, Takeo; Takagi, Kaname
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2114 - 2119
111828-31-0
→
反应条件
88105-10-6
反应条件
1: 69 percent / Triethylamine / ethanol / 2 h / Heating 2: 25 percent / p-Toluenesulfonic acid / ethanol / 2.5 h / Heating View Scheme
参考文献
Takagi, Kaname; Aotsuka, Tomoji; Morita, Hikari; Okamoto, Yoshihisa
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1443 - 1449
109948-71-2
→
反应条件
88105-10-6
反应条件
1: 71 percent / ethanol / 24 h / Ambient temperature 2: 69 percent / Triethylamine / ethanol / 2 h / Heating 3: 25 percent / p-Toluenesulfonic acid / ethanol / 2.5 h / Heating View Scheme
参考文献
Takagi, Kaname; Aotsuka, Tomoji; Morita, Hikari; Okamoto, Yoshihisa
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1443 - 1449
57315-84-1
→
反应条件
88105-10-6
反应条件
1: 75 percent / Triethylamine / ethanol / 0.5 h / Ambient temperature 2: 71 percent / ethanol / 24 h / Ambient temperature 3: 69 percent / Triethylamine / ethanol / 2 h / Heating 4: 25 percent / p-Toluenesulfonic acid / ethanol / 2.5 h / Heating View Scheme
参考文献
Takagi, Kaname; Aotsuka, Tomoji; Morita, Hikari; Okamoto, Yoshihisa
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1443 - 1449
