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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88126-44-7
合成路线
（共 11 条）
130236-63-4
→
反应条件
88126-44-7
反应条件
hydrogen; acetic acid; palladium on activated charcoal in tetrahydrofuran Catalytic hydrogenation; atmospheric pressure;
参考文献
Donnelly, Dervilla M.X.; Finet, Jean-Pierre; Guiry, Patrick J.; Rea, Martin D.
Synthetic Communications, 1999 , vol. 29, # 15 p. 2719 - 2730
1092835-50-1
+
159191-56-7
4-(叔丁基二甲基硅氧基)苯基硼酸
→
反应条件
88126-44-7
反应条件
1: With anhydrous copper acetate in methanol T=28°C; 6 h; Inert atmosphere; 2: With hydrogenchloride in methanol 6 h; Inert atmosphereReflux;
参考文献
Yamamoto, Yoshihiko; Kirai, Naohiro
Organic Letters, 2008 , vol. 10, # 24 p. 5513 - 5516
71597-85-8
4-羟基苯硼酸
+
185418-17-1
→
反应条件
88126-44-7
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); sodium carbonate in methanol; toluene Suzuki coupling; Reflux;
参考文献
Pierson, Jean-Thomas; Dumetre, Aurelien; Hutter, Sebastien; Delmas, Florence; Laget, Michele; Finet, Jean-Pierre; Azas, Nadine; Combes, Sebastien
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 3 p. 864 - 869
6793-92-6
1-苯甲氧基-4-溴苯
→
反应条件
88126-44-7
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C 1.2: tetrahydrofuran / 2 h / -78 °C 2.1: HCl; water / diethyl ether 3.1: 83 percent / copper(I) iodide; sodium carbonate / tetrakis(triphenylphosphane)palladium(0) / benzene; ethanol / 20 h / Heating 4.1: 80 percent / hydrogen; acetic acid / 10 percent palladium on carbon / tetrahydrofuran / atmospheric pressure View Scheme
参考文献
Donnelly, Dervilla M.X.; Finet, Jean-Pierre; Guiry, Patrick J.; Rea, Martin D.
Synthetic Communications, 1999 , vol. 29, # 15 p. 2719 - 2730
146631-00-7
4-苄氧基苯硼酸
→
反应条件
88126-44-7
反应条件
1: 83 percent / copper(I) iodide; sodium carbonate / tetrakis(triphenylphosphane)palladium(0) / benzene; ethanol / 20 h / Heating 2: 80 percent / hydrogen; acetic acid / 10 percent palladium on carbon / tetrahydrofuran / atmospheric pressure View Scheme
参考文献
Donnelly, Dervilla M.X.; Finet, Jean-Pierre; Guiry, Patrick J.; Rea, Martin D.
Synthetic Communications, 1999 , vol. 29, # 15 p. 2719 - 2730
185418-17-1
→
反应条件
88126-44-7
反应条件
1: 83 percent / copper(I) iodide; sodium carbonate / tetrakis(triphenylphosphane)palladium(0) / benzene; ethanol / 20 h / Heating 2: 80 percent / hydrogen; acetic acid / 10 percent palladium on carbon / tetrahydrofuran / atmospheric pressure View Scheme
参考文献
Donnelly, Dervilla M.X.; Finet, Jean-Pierre; Guiry, Patrick J.; Rea, Martin D.
Synthetic Communications, 1999 , vol. 29, # 15 p. 2719 - 2730
2174-64-3
夫拉美诺
→
反应条件
88126-44-7
反应条件
1: 24 mg / HCl gas / ethanol / 48 h 2: 16 mg / methanol; diethyl ether 3: H2 / 10percent Pd/C / ethanol / 4 h / 760 Torr View Scheme
参考文献
Bose; Banerji
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 5 p. 422 - 424
53090-45-2
→
反应条件
88126-44-7
反应条件
1: 24 mg / HCl gas / ethanol / 48 h 2: 16 mg / methanol; diethyl ether 3: H2 / 10percent Pd/C / ethanol / 4 h / 760 Torr View Scheme
参考文献
Bose; Banerji
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 5 p. 422 - 424
130236-62-3
→
反应条件
88126-44-7
反应条件
1: 16 mg / methanol; diethyl ether 2: H2 / 10percent Pd/C / ethanol / 4 h / 760 Torr View Scheme
参考文献
Bose; Banerji
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 5 p. 422 - 424
186581-53-3
重氮甲烷
+
124607-18-7
→
反应条件
74512-60-0
+
88126-44-7
反应条件
in methanol; diethyl ether; chloroform 0.75 h;
参考文献
Monache, Giuliano Delle; Botta, Bruno; Monache, Franco Delle; Botta, Maurizio
Phytochemistry (Elsevier), 1985 , vol. 24, # 6 p. 1355 - 1358
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