6-氯-1-(甲基磺酰基)-1H-吲哚合成路线 （共 5 条）
反应条件
potassium hydroxide in methanol 18 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 49, # 2 p. 249 - 254
反应条件
titanium tetrachloride in toluene
T=110°C; Yield given;
参考文献
Sundberg, Richard J.; Laurino, Joseph P.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 249 - 254
反应条件
sodium hydride in N,N-dimethyl-formamide
T=0 - 20°C;
参考文献
Isaac, Methvin B; Xin, Tao; O'Brien, Anne; St-Martin, David; Naismith, Angela; MacLean, Neil; Wilson, Julie; Demchyshyn, Lidia; Tehim, Ashok; Slassi, Abdelmalik
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 17 p. 2451 - 2454
反应条件
1: 62 percent / NaH / dimethylformamide / 110 °C
2: TiCl4 / toluene / 110 °C
View Scheme
参考文献
Sundberg, Richard J.; Laurino, Joseph P.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 249 - 254
反应条件
1: pyridine / CH2Cl2 / 1) 1 h, 0 deg C; 2) 1 h, 25 deg C
2: 62 percent / NaH / dimethylformamide / 110 °C
3: TiCl4 / toluene / 110 °C
View Scheme
参考文献
Sundberg, Richard J.; Laurino, Joseph P.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 249 - 254
