(3beta,5Xi,9Xi,12beta,17Xi)-20-{[6-O-(beta-D-吡喃葡萄糖基)-beta-D-吡喃葡萄糖基]氧基}-12-羟基达马-24-烯-3-基2-O-[6-O-(羧基乙酰基)-beta-D-吡喃葡萄糖基]-beta-D-吡喃葡萄糖苷合成路线 （共 6 条）
反应条件
1: 110 mg / diethyl ether / 0.5 h / 22 °C 2: 45 mg / β-glucosidase / H2O / 72 h / 37 °C 3: 34 mg / KOH / methanol / 0.5 h / 22 °C View Scheme
参考文献
Kitagawa; Taniyama; Yoshikawa; Ikenishi; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 2961 - 2970
反应条件
1: 110 mg / diethyl ether / 0.5 h / 22 °C 2: 104 mg / 40percent aqueous AcOH / 3 h / 75 °C 3: 45 mg / KOH / methanol / 0.5 h / 20 °C View Scheme
参考文献
Kitagawa; Taniyama; Yoshikawa; Ikenishi; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 2961 - 2970
反应条件
potassium hydroxide in methanol T=22°C; 0.5 h;
参考文献
Kitagawa; Taniyama; Yoshikawa; Ikenishi; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 2961 - 2970
反应条件
potassium hydroxide in methanol T=22°C; 0.5 h; malonic acid determined as its methyl ester by GLC; Product distribution;
参考文献
Kitagawa; Taniyama; Yoshikawa; Ikenishi; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 2961 - 2970
反应条件
potassium hydroxide in methanol T=22°C; 0.5 h; malonic acid determined as its methyl ester by GLC; Product distribution;
参考文献
Kitagawa; Taniyama; Yoshikawa; Ikenishi; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 2961 - 2970
反应条件
1: 110 mg / diethyl ether / 0.5 h / 22 °C 2: 104 mg / 40percent aqueous AcOH / 3 h / 75 °C 3: 45 mg / KOH / methanol / 0.5 h / 20 °C View Scheme
参考文献
Kitagawa; Taniyama; Yoshikawa; Ikenishi; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 2961 - 2970
