反应条件
1.1: 76 percent / BaMnO4 / CH2Cl2 / 20 °C
2.1: BuLi / tetrahydrofuran; hexane / 2 h / -20 °C
2.2: 76 percent / tetrahydrofuran; hexane / -20 - 20 °C
3.1: BaMnO4 / CH2Cl2 / 20 °C
4.1: PPh3 / CH2Cl2 / 0.5 h / 0 °C
4.2: 542 mg / CH2Cl2 / 0.5 h / 0 °C
5.1: 76 percent / BuLi / hexane / 1 h / -78 - 20 °C
6.1: 96 percent / TBAF / tetrahydrofuran / 20 °C
View Scheme
参考文献
Luu, Thanh; Tykwinski, Rik R.
Journal of Organic Chemistry, 2006 , vol. 71, # 23 p. 8982 - 8985
