1: 54 percent / Et3N / CH2Cl2 / 12 h
2: 50 percent / potassium t-butoxide / tetrahydrofuran / 1 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 75 percent / pyridine / 12 h / Ambient temperature
2: 53 percent / PCl5 / CH2Cl2 / 0.08 h
3: 54 percent / Et3N / CH2Cl2 / 12 h
4: 50 percent / potassium t-butoxide / tetrahydrofuran / 1 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266