反应条件
1.1: 77 percent / HNO3; HOAc / 25 °C
2.1: 100 percent / H2 / Pd/C / methanol / 25 °C
3.1: air / acetonitrile / 168 h / 25 °C
3.2: NBS; Na2CO3 / acetonitrile / 25 °C
4.1: 88 percent / NBS; HBr / acetonitrile / 25 °C
5.1: Ni(CO)4 / benzene / 60 °C
5.2: 66 percent / benzene; dimethylformamide / 16 h / 65 °C
6.1: 92 percent / LiAlH4 / diethyl ether / 0.75 h / 25 °C
View Scheme
参考文献
Czerwonka, Regina; Reddy, Kethiri R.; Baum, Elke; Knoelker, Hans-Joachim
Chemical Communications, 2006 , # 7 p. 711 - 713
