phosphorus; hydrogen iodide in acetic acid
T=100°C; 3 h;
参考文献
Jones, David W.; Pomfret, Alan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 13 - 18
lithium aluminium tetrahydride in diethyl ether
T=25°C; 22 h;
参考文献
Jones, David W.; Pomfret, Alan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 13 - 18
1: sodium methoxide / diethyl ether; methanol / 0.08 h / -50 - -40 °C
2: 31 percent / lithium aluminium hydride / diethyl ether / 22 h / 25 °C
View Scheme
参考文献
Jones, David W.; Pomfret, Alan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 13 - 18
1: bromine / CH2Cl2 / 1 h / -14 °C
2: DBU / CH2Cl2 / -50 °C
View Scheme
参考文献
Bradshaw, David P.; Jones, David W.; Nongrum, Firstborn Metthew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 19 - 23
