(R)-(+)-1-(3-甲氧基苯基)乙胺合成路线 （共 22 条）
反应条件
1: PPh3, HN3, DEAD / toluene / 2 h / Ambient temperature 2: H2 / Pd/C / trifluoroacetic acid View Scheme
参考文献
Tetrahedron Letters, , vol. 32, # 49 p. 7175 - 7178
反应条件
solid phase supported Candida antarctica lipase type B in tert-butyl methyl ether T=30°C; 120 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 15 p. 5304 - 5310
反应条件
1: toluene; diethyl ether / 0.42 h / -20 °C 2: 72 percent / Mo(CO)6 / acetonitrile; H2O / 1 h / 85 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 17 p. 5595 - 5607
反应条件
1: 99 percent / TsOH / toluene / 0.5 h / Heating 2: toluene; diethyl ether / 0.42 h / -20 °C 3: 72 percent / Mo(CO)6 / acetonitrile; H2O / 1 h / 85 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 17 p. 5595 - 5607
反应条件
hydrogenchloride; water in methanol T=20°C;
参考文献
Applied Organometallic Chemistry, , vol. 25, # 2 p. 105 - 109
反应条件
2: OH(-), H2O View Scheme
参考文献
Chemical Communications, , # 21 p. 2415 - 2416
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 24 h / Cooling with ice 1.2: 20 °C 2.1: C5H12BNO / tetrahydrofuran / 24 h / 20 °C 2.2: 24 h / Reflux View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 23, # 9 p. 716 - 721
反应条件
(R)-(6-methoxy-2-naphthyl)glycolic acid in ethanol; water Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 23 p. 3807 - 3813
反应条件
water; hydroxide Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 21 p. 2415 - 2416
反应条件
1: (1R,2S)-N-benzylephedrine / toluene / 48 h / Inert atmosphere 2: hydrogenchloride; water / methanol / 20 °C View Scheme
参考文献
Applied Organometallic Chemistry, , vol. 25, # 2 p. 105 - 109
