1: diphenyldisulfane With aluminium trichloride; zinc in water; acetonitrile
T=65°C; 1.5 h;
2: cyclopent-2-enone With aluminium trichloride in water; acetonitrile
T=65°C; Michael addition; 1.5 h; Further stages.;
参考文献
Movassagh, Barahman; Zakinezhad, Yousef
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 1 p. 47 - 49
ammonium hydroxide; zinc in 1,4-dioxane
Michael Addition; 24 h; Schlenk techniqueRefluxInert atmosphere; Overall yield = 83 percent; diastereoselective reaction;
参考文献
Loren Nunes, Vanessa; De Oliveira, Ingryd Cristina; Soares Do Rego Barros, Olga
European Journal of Organic Chemistry, 2014 , vol. 2014, # 7 p. 1525 - 1530