1: trimethylsilylacetylene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.25 h;
2: diphenyldisulfane in tetrahydrofuran; hexane
T=-78 - 20°C; 2 h; Inert atmosphereSchlenk technique;
参考文献
Nitsch, Dominik; Huber, Stefan M.; Poethig, Alexander; Narayanan, Arjun; Olah, George A.; Prakash, G. K. Surya; Bach, Thorsten
Journal of the American Chemical Society, 2014 , vol. 136, # 7 p. 2851 - 2857