2,3,6,7-四(硫代苯甲酰基)四硫杂富瓦烯合成路线 （共 6 条）
反应条件
1: sodium tert-butyl sulfide / dimethylformamide / 0.25 h 2: 0.25 h View Scheme
参考文献
Khodorkovskii, V. Yu.; Katsen, Ya. Ya.; Neiland, O. Ya.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 7 p. 1442
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 7 p. 1582 - 1583
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile
0.25 h;
参考文献
Hansen, Thomas K.; Bryce, Martin R.; Howard, Judith A. K.; Yufit, Dimitri S.
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5324 - 5327
反应条件
dicobalt octacarbonyl in benzene
3 h; Heating;
参考文献
Hansen, Thomas K.; Hawkins, Ian; Varma, K. Sukumar; Edge, Stephen; Larsen, Sine; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 1963 - 1966
反应条件
1: 89 percent / HBF4 / diethyl ether / 0.33 h
2: 82 percent / diisopropylethylamine / acetonitrile / 0.25 h
View Scheme
参考文献
Hansen, Thomas K.; Bryce, Martin R.; Howard, Judith A. K.; Yufit, Dimitri S.
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5324 - 5327
反应条件
1: 65 percent / CH2Cl2 / 3 h
2: 82 percent / diisopropylethylamine / acetonitrile / 0.25 h
View Scheme
参考文献
Hansen, Thomas K.; Bryce, Martin R.; Howard, Judith A. K.; Yufit, Dimitri S.
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5324 - 5327
反应条件
1: 89 percent / HBF4 / diethyl ether / 0.33 h
2: 82 percent / diisopropylethylamine / acetonitrile / 0.25 h
View Scheme
参考文献
Hansen, Thomas K.; Bryce, Martin R.; Howard, Judith A. K.; Yufit, Dimitri S.
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5324 - 5327
