4-(2-(3,4-二甲氧基苄基氨基)乙基)苯酚合成路线 （共 6 条）
反应条件
1: 3 Angstroem molecular sieves
2: 100 percent / H2 / Pd/C / tetrahydrofuran / 1.17 h / 25 °C / 15001.2 Torr
View Scheme
参考文献
Saaby, Steen; Knudsen, Kristian Rahbek; Ladlow, Mark; Ley, Steven V.
Chemical Communications, 2005 , # 23 p. 2909 - 2911
反应条件
1: 3 Angstroem molecular sieves
2: 100 percent / H2 / Pd/C / tetrahydrofuran / 1.17 h / 25 °C / 15001.2 Torr
View Scheme
参考文献
Saaby, Steen; Knudsen, Kristian Rahbek; Ladlow, Mark; Ley, Steven V.
Chemical Communications, 2005 , # 23 p. 2909 - 2911
反应条件
1: in methanol
T=20°C; 6 h;
2: With sodium tetrahydroborate in methanol
T=20°C; 4 h; Further stages.;
参考文献
Kodama, Sumiaki; Takita, Hirofumi; Kajimoto, Tetsuya; Nishide, Kiyoharu; Node, Manabu
Tetrahedron, 2004 , vol. 60, # 22 p. 4901 - 4907
反应条件
polymer supported borohydride reagent in methanol
Yield given;
参考文献
Ley, Steven V.; Schucht, Olivier; Thomas, Andrew W.; Murray, P. John
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1251 - 1252
反应条件
1: 100 percent / polymer supported perruthenate reagent / CH2Cl2
3: polymer supported borohydride reagent / methanol
View Scheme
参考文献
Ley, Steven V.; Schucht, Olivier; Thomas, Andrew W.; Murray, P. John
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 10 p. 1251 - 1252
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Han, Sun-Young; Kitahata, Nobutaka; Saito, Tamio; Kobayashi, Masatomo; Shinozaki, Kazuo; Yoshida, Shigeo; Asami, Tadao
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 12 p. 3033 - 3036
