chromium(VI) oxide in water; acetic acid
T=65°C; 0.75 h;
参考文献
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152
1: 50 percent / tetrahydrofuran; diethyl ether / 0.5 h / Heating
2: 28 percent / chromium trioxide / acetic acid; H2O / 0.75 h / 65 °C
View Scheme
参考文献
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152
1: 50 percent / tetrahydrofuran; diethyl ether / 0.5 h / Heating
2: 28 percent / chromium trioxide / acetic acid; H2O / 0.75 h / 65 °C
View Scheme
参考文献
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152
1: 95 percent / lithium aluminium hydride / tetrahydrofuran / 4 h / Ambient temperature
2: 77 percent / activated manganese dioxide / CHCl3 / 30 h / Heating
3: 50 percent / tetrahydrofuran; diethyl ether / 0.5 h / Heating
4: 28 percent / chromium trioxide / acetic acid; H2O / 0.75 h / 65 °C
View Scheme
参考文献
Giles, Robin G. F.; Mitchell, Peter R. K.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2147 - 2152