反应条件
1: 2-methyl-thiophene With n-butyllithium in diethyl ether; hexane
T=0°C; 1.5 h; Inert atmosphereSchlenk technique;
2: indole-2,3-dione in diethyl ether; hexane
T=20°C; 6 h; Inert atmosphereSchlenk technique;
3: With lithium aluminium tetrahydride in diethyl ether; hexane
3 h; RefluxInert atmosphereSchlenk technique;
参考文献
Nagase, Yuta; Shirai, Hiroyuki; Kaneko, Masayoshi; Shirakawa, Eiji; Tsuchimoto, Teruhisa
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1456 - 1459