(S)-2,3-二氢苯并[1,4]二氧六环-2-甲酸乙酯合成路线 （共 3 条）
反应条件
whole cells of Arthrobacter sp. ABL MTCC No. 5125 lipase in aq. phosphate buffer; butan-1-ol
T=25°C; pH=7.1; 4 h; enantioselective reaction;
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
1: bromine / tetrachloromethane / 2 h / 0 - 60 °C
2: potassium carbonate / acetone / 18 h / |Reflux
3: whole cells of Arthrobacter sp. ABL MTCC No. 5125 lipase / aq. phosphate buffer; butan-1-ol / 4 h / 25 °C / pH 7.1
View Scheme
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
反应条件
1: potassium carbonate / acetone / 18 h / |Reflux
2: whole cells of Arthrobacter sp. ABL MTCC No. 5125 lipase / aq. phosphate buffer; butan-1-ol / 4 h / 25 °C / pH 7.1
View Scheme
参考文献
Rouf, Abdul; Gupta, Pankaj; Aga, Mushtaq A.; Kumar, Brijesh; Chaubey, Asha; Parshad, Rajinder; Taneja, Subhash C.
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1615 - 1623
