N-(3-羟丙基)酞亚胺合成路线 （共 19 条）
反应条件
triethylamine in toluene T=130°C; 3 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 18, # 16 p. 5903 - 5914
反应条件
18-crown-6 ether in toluene T=104°C;
参考文献
Tetrahedron Letters, , vol. 34, # 24 p. 3919 - 3920
反应条件
silver hexafluoroantimonate; phloroglucinol trimethyl ether in dichloromethane T=40°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 77, # 20 p. 9227 - 9235,9
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
US5681966 A1, ;
US 5681966 A
反应条件
triethylamine in tetrahydrofuran 6 h; Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 42, # 4 p. 706 - 721
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
US6201016 B1, ;
US5681966 A1, ;
US 5681966 A
反应条件
in N,N-dimethyl-formamide T=90°C; 18 h; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 52, # 22 p. 7029 - 7043
反应条件
in dichloromethane; toluene
参考文献
US4652573 A1, ;
US 4652573 A
反应条件
potassium hydroxide engt die von Kaliumbromid abfiltrierte Fluessigkeit ein und erhitzt den entstandenen Phthalsaeure-mono-<γ-amino-propylester> ueber den Schmelzpunkt;
参考文献
Chemische Berichte, , vol. 38, p. 633,2389
Chemische Berichte, , vol. 23, p. 89
反应条件
1: With diisopropyl-carbodiimide; copper(II) bis(trifluoromethanesulfonate) in tetrahydrofuran T=100°C; 0.0833333 h; microwave irradiation; 2: With acetyl-bromide in tetrahydrofuran T=150°C; 0.0833333 h; microwave irradiation; Further stages.;
参考文献
Crosignani, Stefano; Nadal, Brice; Li, Zhengning; Linclau, Bruno
Chemical Communications, 2003 , # 2 p. 260 - 261
