3-(叔-丁基)-1-甲基萘合成路线 （共 5 条）
反应条件
sulfur
T=230 - 270°C; 1.58333 h;
参考文献
Jackson, Richard A.; Rhodes, Christopher J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 53 - 57
反应条件
1: 23 percent / ZnCl2 / 6 h / 75 - 110 °C
2: 20 percent / glacial AcOH, 85percent H3PO4, concd HCl / 6 h / Heating
3: 98 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating
4: 75 percent / sulfur / 1.58 h / 230 - 270 °C
View Scheme
参考文献
Jackson, Richard A.; Rhodes, Christopher J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 53 - 57
反应条件
1: 20 percent / glacial AcOH, 85percent H3PO4, concd HCl / 6 h / Heating
2: 98 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating
3: 75 percent / sulfur / 1.58 h / 230 - 270 °C
View Scheme
参考文献
Jackson, Richard A.; Rhodes, Christopher J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 53 - 57
反应条件
1: 98 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating
2: 75 percent / sulfur / 1.58 h / 230 - 270 °C
View Scheme
参考文献
Jackson, Richard A.; Rhodes, Christopher J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 53 - 57
参考文献
Dimroth,K. et al.
Justus Liebigs Annalen der Chemie, 1964 , vol. 678, p. 202 - 213
