3-羟基-2-萘甲酸甲酯合成路线 (共 89 条)
反应条件
N-phenyl-N-β-naphthylamine; tert-butylamine in methanol
72 h; Ambient temperature;
参考文献
Smrcina, Martin; Vyskocil, Stepan; Maca, Bohumil; Polasek, Miroslav; Claxton, Thomas A.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2156 - 2163
反应条件
tert-butylamine in methanol
72 h; Ambient temperature;
参考文献
Smrcina, Martin; Vyskocil, Stepan; Maca, Bohumil; Polasek, Miroslav; Claxton, Thomas A.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2156 - 2163
反应条件
tert-butylamine; copper dichloride in methanol
T=50°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hovorka; Scigel; Gunterova; Tichy; Zavada
Tetrahedron, 1992 , vol. 48, # 43 p. 9503 - 9516
反应条件
tert-butylamine in methanol
72 h; Ambient temperature;
参考文献
Smrcina, Martin; Vyskocil, Stepan; Maca, Bohumil; Polasek, Miroslav; Claxton, Thomas A.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2156 - 2163
反应条件
oxygen; copper(l) chloride; (-)-sparteine
T=20°C; 5 h;
参考文献
Temma, Tomohisa; Habaue, Shigeki
Tetrahedron Letters, 2005 , vol. 46, # 34 p. 5655 - 5657
反应条件
1: LiAlH4; diethyl ether
2: copper oxide-chromium oxide catalyst; ethanol / 140 °C / 147102 Torr / Hydrogenation
View Scheme
参考文献
Miller et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 296
反应条件
tert-butylamine; copper dichloride in methanol
T=50°C; 1.83333 h; Yields of byproduct given;
参考文献
Hovorka; Scigel; Gunterova; Tichy; Zavada
Tetrahedron, 1992 , vol. 48, # 43 p. 9503 - 9516
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Zhang, Jianghua; Gao, Xinqin; Zhang, Chengyi; Ma, Jianfei; Zhao, Defeng
Synthetic Communications, 2009 , vol. 39, # 9 p. 1640 - 1654
反应条件
(+)-1,2,3,4,1',2',3',4'-octahydro-1,1'-bisisoquinoline; copper dichloride in acetonitrile
T=20°C; 27 h;
参考文献
Illesinghe, Jayamini; Ebeling, Richard; Ferguson, Brett; Patel, Jim; Campi, Eva M.; Jackson, W. Roy; Robinson, Andrea J.
Australian Journal of Chemistry, 2004 , vol. 57, # 2 p. 167 - 176
反应条件
tert-butylamine; copper dichloride in methanol
T=41°C; 2 h; Yields of byproduct given;
参考文献
Hovorka; Scigel; Gunterova; Tichy; Zavada
Tetrahedron, 1992 , vol. 48, # 43 p. 9503 - 9516