3-羟基-2-萘甲酸甲酯合成路线 （共 89 条）
反应条件
tert-butylamine in methanol
72 h; Ambient temperature;
参考文献
Smrcina, Martin; Vyskocil, Stepan; Maca, Bohumil; Polasek, Miroslav; Claxton, Thomas A.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2156 - 2163
反应条件
tert-butylamine; copper dichloride in methanol
T=50°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hovorka; Scigel; Gunterova; Tichy; Zavada
Tetrahedron, 1992 , vol. 48, # 43 p. 9503 - 9516
反应条件
tert-butylamine in methanol
72 h; Ambient temperature;
参考文献
Smrcina, Martin; Vyskocil, Stepan; Maca, Bohumil; Polasek, Miroslav; Claxton, Thomas A.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2156 - 2163
反应条件
oxygen; copper(l) chloride; (-)-sparteine
T=20°C; 5 h;
参考文献
Temma, Tomohisa; Habaue, Shigeki
Tetrahedron Letters, 2005 , vol. 46, # 34 p. 5655 - 5657
反应条件
1: 60 percent / 40percent aq NaOH / acetone / Heating
2: 10percent KOH / methanol / 0.5 h / Heating
3: 0.17 h / Heating
View Scheme
参考文献
Bergmann; Berlin
Journal of Organic Chemistry, 1938 , vol. 3, p. 246,249
反应条件
1: 60 percent / 40percent aq NaOH / acetone / Heating
2: 10percent KOH / methanol / 0.5 h / Heating
3: 0.17 h / Heating
4: 40 percent / NH2NH2*H2O / methanol / Heating
View Scheme
参考文献
Prajer-Janczewska, Lidia; Wroblewski, Juliusz
Polish Journal of Chemistry, 1980 , vol. 54, # 7/8 p. 1431 - 1437
反应条件
tert.-butylhydroperoxide in decane; acetonitrile
T=70°C; 6.5 h; Catalytic behavior; regioselective reaction;
参考文献
Khatri, Praveen K.; Jain, Suman L.
Catalysis Letters, 2012 , vol. 142, # 8 p. 1020 - 1025
反应条件
amidation; 0.25 h; Heating;
参考文献
Griffiths, John; Feng, Kai-Chia
Journal of Materials Chemistry, 1999 , vol. 9, # 10 p. 2333 - 2338
参考文献
Kalle and Co.
Patent: DE896453 , 1949 ;
反应条件
1: 20 percent / NaH / tetrahydrofuran / 48 h / Heating
2: 68 percent / aq. NaOH / ethanol / 4 h / Heating
View Scheme
参考文献
Kang, Sang Ihn; Czech, Anna; Czech, Bronislaw; Stewart, Louis E.; Bartsch, Richard A.
Analytical Chemistry, 1985 , vol. 57, p. 1713 - 1717
