3-羟基-2-萘甲酸甲酯合成路线 （共 89 条）
反应条件
potassium carbonate in acetonitrile
48 h; Heating;
参考文献
Ashram, Muhammad
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2005 , vol. 60, # 8 p. 891 - 900
反应条件
methanol; nickel
T=150°C; P=56634.1 Torr; Hydrogenation;
参考文献
Hunsberger et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3294,3299
反应条件
sulfuric acid; nitric acid in dichloromethane
T=0°C; 0.25 h;
参考文献
Xie, Fuchun; Li, Bingbing X.; Xiao, Xiangshu
Letters in Organic Chemistry, 2013 , vol. 10, # 5 p. 380 - 384
反应条件
1: 91 percent / Cs2CO3 / 32 h / Heating
2: 93 percent / LiAlH4 / tetrahydrofuran / 3 h / 20 °C
3: 92 percent / 4-methylmorpholine N-oxide; tetrapropylammonium perruthenate / CH2Cl2
View Scheme
参考文献
Wu, Kun-Chan; Lin, Yu-Shan; Yeh, Yu-Shan; Chen, Chun-Yen; Ahmed, Moawia O.; Chou, Pi-Tai; Hon, Yung-Son
Tetrahedron, 2004 , vol. 60, # 51 p. 11861 - 11868
反应条件
sodium hydroxide; acetone
Erhitzen des Reaktionsprodukts unter vermindertem Druck;
参考文献
Bergmann; Berlin
Journal of Organic Chemistry, 1938 , vol. 3, p. 246,249
Full Text Show Details
Wystrach; Tarbell
Journal of the American Chemical Society, 1943 , vol. 65, p. 2472
反应条件
1: 60 percent / 40percent aq NaOH / acetone / Heating
2: 180 - 190 °C / 5 - 7 Torr
View Scheme
参考文献
Prajer-Janczewska, Lidia; Wroblewski, Juliusz
Polish Journal of Chemistry, 1980 , vol. 54, # 7/8 p. 1431 - 1437
反应条件
1: 89 percent / potassium carbonate; 18-crown-6 ether / acetone / 12 h / Heating
2: 87 percent / LiAlH4 / tetrahydrofuran / 6 h / 20 °C
3: 82 percent / pyridinium chlorochromate; sodium acetate; molecular sieves 4 Angstroem / CH2Cl2 / 0.67 h
4: 80 percent / BBr3 / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Wu, Kun-Chan; Lin, Yu-Shan; Yeh, Yu-Shan; Chen, Chun-Yen; Ahmed, Moawia O.; Chou, Pi-Tai; Hon, Yung-Son
Tetrahedron, 2004 , vol. 60, # 51 p. 11861 - 11868
反应条件
1: diethyl ether / 1.5 h / Heating
2: 96 percent / sodium acetate / 7 h / Heating
3: 10.366 g / H2 / Pd/C / methanol / 17 h / Ambient temperature
View Scheme
参考文献
Matsumoto, Takashi; Imai, Sachihiko; Yamamoto, Naoya
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 911 - 920
反应条件
sodium hydride
1.) 70-80 deg C, 6 h 2.) room temperature, 0.5 h;
参考文献
Cremins, Peter J.; Saengchantara, Suthiweth T.; Wallace, Timothy W.
Tetrahedron, 1987 , vol. 43, # 13 p. 3075 - 3082
