1: With triethylsilane; triphenylmethylium tetrakis(pentafluorophenyl)borate in 1,2-dichloro-benzene T=20°C; 16 h; Schlenk techniqueInert atmosphere; 2: With water in 1,2-dichloro-benzene Schlenk techniqueInert atmosphere; Reagent/catalyst;

tetramethylene sulfide; diethylzinc in dichloromethane; toluene T=20°C; 16 h;

暂无反应条件数据

(i) aq. HCl, (ii) /BRN= 607898/, NaOH; Multistep reaction;