[1-(4-氨基苯磺酰基)哌啶-4-基]氨基甲酸叔丁酯合成路线 （共 3 条）
反应条件
iron; ammonium chloride in ethanol; water
T=80°C; 3 h;
参考文献
Prime, Michael; Courtney, Stephen Martin; Marston, Richard; Dominguez, Celia; Macdonald, Douglas; Wityak, John
Patent: US2012/302539 A1, 2012 ;
Location in patent: Page/Page column 100 ;
US 20120302539 A1
反应条件
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
2: ammonium chloride; iron / ethanol; water / 3 h / 80 °C
View Scheme
参考文献
Prime, Michael; Courtney, Stephen Martin; Marston, Richard; Dominguez, Celia; Macdonald, Douglas; Wityak, John
Patent: US2012/302539 A1, 2012 ;
US 20120302539 A1
反应条件
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
2: ammonium chloride; iron / ethanol; water / 3 h / 80 °C
View Scheme
参考文献
Prime, Michael; Courtney, Stephen Martin; Marston, Richard; Dominguez, Celia; Macdonald, Douglas; Wityak, John
Patent: US2012/302539 A1, 2012 ;
US 20120302539 A1
