2,2-二(1H-吲哚-3-基)乙基乙酸酯合成路线 （共 15 条）
反应条件
1: 68 percent / LiAlH4 / diethyl ether / 24 h / 20 °C
2: 85 percent / pyridine
View Scheme
参考文献
Sato, Shingo; Sato, Toshihiro
Carbohydrate Research, 2005 , vol. 340, # 14 p. 2251 - 2255
反应条件
1: 100 percent / ethyl acetate; diethyl ether
2: 68 percent / LiAlH4 / diethyl ether / 24 h / 20 °C
3: 85 percent / pyridine
View Scheme
参考文献
Sato, Shingo; Sato, Toshihiro
Carbohydrate Research, 2005 , vol. 340, # 14 p. 2251 - 2255
反应条件
1: 72 percent / LiAlH4 / diethyl ether / 1 h / 20 °C
2: 98 percent / Mg(ClO4)2 / diethyl ether / 1 h / 20 °C
View Scheme
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Foglia, Gioia; Giuliani, Arianna; Marcantoni, Enrico; Sambri, Letizia
Synthesis, 2004 , # 6 p. 895 - 900
反应条件
trifluoroacetic acid in acetonitrile
25 h; Ambient temperature;
参考文献
Singh
Tetrahedron, 1988 , vol. 44, # 18 p. 5897 - 5904
反应条件
toluene-4-sulfonic acid
Yield given. Multistep reaction;
参考文献
Osawa, Toshihiko; Namiki, Mitsuo
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4719 - 4722
